Author(s): Xinyuan Xu, Chungui Wang, Zhenghong Zhou, Zebing Zeng, Xinpeng Ma, Guofeng Zhao and Chuchi Tang
Page: [640 - 642] Pages: 3
* (Excluding Mailing and Handling)
Thermal condensation of acetals with different thiophosphoramides at 120-160 °C resulted in the formation of the corresponding N-thiophosphoryl imines in good to excellent yield (80-98%) with high purity ( > 95%, determined by 1H NMR and elemental analyses).
Keywords: N-Thiophosphoryl imine, thermal condensation, thiophosphoramide, acetal
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